KMID : 0385520120250040236
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Analytical Science & Technology 2012 Volume.25 No. 4 p.236 ~ p.241
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Determination of hazardous semi-volatile organic compounds in industrial wastewater using disk-type solid-phase extraction and GC-MS
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Lee In-Jung
Im Tae-Hyo Heo Seong-Nam Nam Su-gyeong Cheon Se-Uk Lee Jae-gwan
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Abstract
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There are many industrial factories in the central Nakdong river basin and have been occurred water pollution accidents by hazardous chemicals such as phenol, 1,4-dioxane and perchlorate. In this study, ten compounds of semi-volatile organic compounds (SVOCs) (dichlorvos, toluene-2,4-diisocyanate, 4,4'-methylenedianiline, 4,4'-methylenebis (2-chloroaniline), diethyl phthalate, di-n-butyl phthalate, butyl benzyl phthaltate, bis (2-ethylhexyl) adipate, benzophenone, 4,4'-bisphenol A) of hazardous chemicals which may be potentially discharged into the Nakdong river, were determined by gas chromatography-mass spectrometry (GC-MS) with disk-type solid-phase extraction. Accuracy and precision were in the range of 75.6~110.5%, and 4.6~12.7%, respectively and recovery was in the range of 72.4~127.9%. Three compounds (bis (2-ethylhexyl)adipate, benzophenone, 4,4'-bisphenol A) were detected in industrial wastewater such as wastewater treatment plants (WWTPs) and wastewater discharge facilities in the Nakdong River basin.
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KEYWORD
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SVOCs, GC-MS, disk-type solid phase extraction, industrial wastewater
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